Physical contaminants (or ‘foreign bodies’) are objects such as hair, plant stalks or pieces of plastic/metal that can occur as contaminants in food. Sometimes the object is a natural component of the food (e.g. a fruit stalk) - but in all cases it is important to find out what it is and how and when it got there.
X-ray microanalysis in the scanning electron microscope is used to gain an elemental composition of a glass fragment. This composition is then interpreted to identify a specific type of glass such as soda-lime glass, heat-resistant glass and float glass. See sample report.
FT-IR spectroscopy is performed on plastic samples to gain a spectrum of infrared absorption. This is then compared against a vast database of reference spectra to identify the material. Some commonly identified plastics are PVC, polyethylene, polycarbonate, polysulfone, polypropylene and polystyrene. See sample report.
X-ray microanalysis in the scanning electron microscope is used to gain an elemental composition of metal. The suite of elements within a sample can distinguish between different types of metal such as steel, stainless steel, stainless steel type 316, nickel-plated steel, galvanised steel and corroded steel. See sample report.
Suspected bone samples can be confirmed by examination under the compound microscope for pore-like structures consistent with bone, known as lacunae. This is followed by X-ray microanalysis in the scanning electron microscope to determine the elemental composition of the sample. Large peaks of phosphorous and calcium within the spectrum are indicative of bone. See sample report.
Suspected pharmaceutical samples can be analysed by our chromatography team using gas chromatography and liquid chromatography to look for peaks
of interest which may be consistent with an active ingredient, such as amoxicillin which is used in antibiotics.
The microscopy section can also use FT-IR spectroscopy in combination with an identification database and compound microscopy to try and determine the type of capsule shell and in some cases the presence of chemical compounds, fillers and active ingredients found within pharmaceutical products. See sample report.
Suspected insects can be examined under the stereo microscope to identify features such as legs, antennae and wings. Samples which require speciation can then be sent off for further analysis to expert entomologists at one of our approved subcontractors, who will aim to provide an identification. In some cases, the experts are able to advise on typical geographical distributions and life cycles of insects. A chemical test known as a phosphatase test can also be carried out by the microscopy section, which aims to identify whether the phosphatase enzyme within a once-living sample, such as an insect, is still active or if it has been denatured though heat treatment/cooking. Please note, samples which are mouldy may not be suitable for phosphatase analysis as the mould will also naturally produce the phosphatase enzyme and may give a false positive result. See sample report.
Plant matter / wood
Sectioning, staining and examination under the compound microscope of suspected plant matter can reveal cell types and structures which may be indicate a specific source. Wood samples can also be sectioned, stained and examined under the compound microscope, which can reveal features consistent with various species of hardwoods, softwoods and woody monocots. In addition, we have a reference collection of woods within our database which can assist with comparing features seen within complaint samples with those found in known samples to identify a likely source. See sample report.
Sectioning, staining and examination under a compound microscope is used to identify features consistent with tissues from an animal such as muscle fibres, adipose tissue, elastin fibre, collagen and cartilage. In some cases, FT-IR spectroscopy is also used to gain an infrared absorption spectrum of a sample, which may produce a spectrum consistent with organic matter with bands consistent with protein. See sample report.
X-ray microanalysis is used to determine the elemental composition of the sample. Silicate minerals will contain high levels of silicon and oxygen. In some cases, a large peak of aluminium will also be seen, indicating an alumino-silicate mineral. See sample report.
Features common to hairs are assessed under a compound microscope (and used to identify potential sources). These features include the scale pattern, the medulla and the shape of the root, tip and shaft. These structures can aid in the identification of the hair as human (and the potential location on the body) or animal and if animal the possible species. See sample report.
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Where we refer to UKAS Accreditation
Campden BRI (Chipping Campden) Limited is a UKAS accredited testing laboratory No. 1079 Campden BRI (Nutfield) is a UKAS accredited testing laboratory No. 1207